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X-Ray K-Absorption Fine Structure Studies of Some Copper(II) Mixed-Ligand Complexes with Alanine as Primary Ligand

✍ Scribed by Ashutosh Mishra; P. A. Kekre; Rajesh Dubey; B. D. Shrivastava

Publisher: John Wiley and Sons
Year: 1997
Tongue: English
Weight: 259 KB
Volume: 26
Category: Article
ISSN: 0049-8246
DOI: 10.1002/(sici)1097-4539(199703)26:2<75::aid-xrs192>3.0.co;2-v

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✦ Synopsis

X-ray absorption Ðne structure studies of some structurally important copper(II) mixed-ligand complexes were carried out in the solid state and in aqueous solution. The analysis of the Ðne structure data gave the average bond lengths and provided useful information about the environment of the absorbing atom, the phase parameters of the Ðrst coordination shell and the total phase shift.

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Edge shifts (1E ), effective nuclear charge (Z eff ) and % covalency for some copper(II) mixed-ligand complexes were determined by investigating the copper K-absorption edge using a Seifert x-ray generator and a 0.4 m Cauchois-type bent crystal transmission spectrograph. The shift values are suggest