Study of an amorphous phase in plasma-sprayed hydroxyapatite (HA) coatings is important owing to its unique characteristics and nonnegligible amount of the amorphous phase compared to crystalline HA. However, little is known about the component parts of an amorphous phase. It is known that amorphous
X-ray diffraction studies on plasma-sprayed calcium phosphate-coated implants
β Scribed by Koch, B. ;Wolke, J. G. C. ;de Groot, K.
- Publisher
- John Wiley and Sons
- Year
- 1990
- Tongue
- English
- Weight
- 782 KB
- Volume
- 24
- Category
- Article
- ISSN
- 0021-9304
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β¦ Synopsis
Calcium phosphate coatings on steel, obtained by the plasma-spray technique, were examined by x-ray diffraction in order to get some information on their crystallographic structure and crystallinity. Surface roughness values were also determined. These coatings are of interest for hip-prosthesis materials in particular.
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## Abstract Factors involved with the plasmaβspray coating procedure, such as starting powder compound (fluorapatite, hydroxylapatite, magnesiumβwhitlockite, or tetraβcalcium phosphate), powder particle distribution 1β45 or 1β125 (ΞΌm), powder port gun (port 2 or 6), and postβheat treatment of 1 h a
A method to measure the amorphous calcium phosphate (ACP) content of plasma sprayed hydroxyapatite (HA) coatings is presented. The areas of the crystalline peaks and the broad amorphous "hump" in an X-ray diffraction scan of a mixture of crystalline and amorphous HA can be fitted using conventional
Several factors playing a possible role in determining coating stability and bone tissue response were studied in in vivo experiments. These factors involving the plasmaspray coating procedure were as follows: 1) plasmaspray powder port 2 or 6; 2) particle size distribution; 3) hydroxylapatite versu
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