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X-ray diffraction refinement of the crystal structure of anosovite prepared from leucoxene

✍ Scribed by V. Grass; P. Istomin; L. Nazarova

Publisher: John Wiley and Sons
Year: 2009
Tongue: English
Weight: 228 KB
Volume: 44
Category: Article
ISSN: 0232-1300
DOI: 10.1002/crat.200800213

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✦ Synopsis

The crystal structure of anosovite, (Ti 1.69 Al 0.26 Fe 0.05 ) 3+ (Ti 0.97 Zr 0.03 ) 4+ O 5 , prepared by carbothermal reduction of leucoxene under vacuum at 1450°C has been refined by Rietveld method using powder X-ray diffraction data. It was found that it represents slightly monoclinically deformed pseudobrookite type structure with lattice parameters a = 9.8111 Å, b = 3.7509 Å, c = 9.9468 Å, β = 90.628°.

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