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X-ray diffraction analysis of barton oxides

✍ Scribed by A. de la Torre; M. Torralba; A. García; P. Adeva

Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
972 KB
Volume
15
Category
Article
ISSN
0378-7753

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✦ Synopsis

In consequence of the influence of the composition of Barton oxides on the behaviour of batteries, a method has been developed for the quantitative determination of orthorhombic and tetragonal monoxides.

An X-ray diffraction, internal standard method was used. Factors such as diffraction peak overlapping and its method of measurement, type of radiation, particle size as a function of the mass absorption coefficient, and the wavelength used, were all taken into account.

An operational method was established and a statistical error analysis was carried out. Although the error varies with both chemical species and concentration, it can be considered as acceptable.

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✍ P. Ruiz; B. Delmon 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 308 KB

X-ray diffraction analyses were carried out by nine laboratories. The equipment and experimental conditions of analysis were generally different. However, the results obtained were very similar and coherent. Samples with a high vanadium content showed exclusively the presence of TiOz (anatase) and c