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X-ray crystal structures of twocis-Mo(CO)4{(Ph2PO)2P(O)R} (R=Me, MeO-p-C6H4) complexes with unusual Mo-PPh2-O-P(O)R-O-PPh2chelate rings

✍ Scribed by Gary M. Gray; Yalin Zhang

Publisher
Springer
Year
1993
Tongue
English
Weight
423 KB
Volume
23
Category
Article
ISSN
1572-8854

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Photolysis of the cis-Mo(CO) 4 {Ph 2 P(CH 2 CH 2 O) n CH 2 CH 2 PPh 2 -P,P%}, (1, n= 3; 2, n= 4; 3, n= 5) metallacrown ethers in tetrahydrofuran under nitrogen gives moderate yields of the corresponding trans-Mo(CO) 4 {Ph 2 P(CH 2 CH 2 O) n CH 2 CH 2 PPh 2 -P,P%} (4, n =3; 5, n= 4; 6, n= 5) metallac