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Visible-light-mediated conversion of alcohols to halides

โœ Scribed by Dai, Chunhui; Narayanam, Jagan M. R.; Stephenson, Corey R. J.

Book ID
109913133
Publisher
Nature Publishing Group
Year
2011
Tongue
English
Weight
807 KB
Volume
3
Category
Article
ISSN
1755-4330

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The conversion of alcohols to halides using a filterable phosphine source
โœ Michael P Pollastri; John F Sagal; George Chang ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 60 KB

The conversion of primary and secondary alcohols to chlorides and bromides using 1,2-bis(diphenylphosphino)ethane (diphos) is described. Use of this reagent in lieu of the typical triphenylphosphine-carbontetrahalide complex provides a facile means of purifying the desired halide from the phosphine-