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Vibrational spectroscopy and theoretical studies on 2,4-dinitrophenylhydrazine

✍ Scribed by V. Chiş; S. Filip; V. Miclăuş; A. Pîrnău; C. Tănăselia; V. Almăşan; M. Vasilescu

Book ID
104058278
Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
106 KB
Volume
744-747
Category
Article
ISSN
0022-2860

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A novel D3T derivative, 5-amino-4-cyano-3H-1,2-dithiole-3-thione (compound 1) has been obtained in one-pot reaction. The crystal is orthorhombic, space group Pbca, with a = 10.3667(4) A ˚, b = 10.8898(4) A ˚, c = 11.4942(5) A ˚, V = 1297.60(9) A ˚3, and Z = 8. In the crystal, molecules are firstly s