Variation in Physiological Activity of Alcohols Among Isomers and Homologs*

✍ Scribed by Hufferd, Ralph W.

• Book ID: 102423545
• Publisher: Elsevier
• Year: 1932
• Weight: 385 KB
• Volume: 21
• Category: Article
• ISSN: 0898-140X
• DOI: 10.1002/jps.3080210605

✦ Synopsis

The refractometer used is of the Abbe type and gave the values 1.3331 and All physical properties used for comparison were taken from "International Anschutz thermometers corrected to *0.2" were used. All boiling points B. P. 64.5", N z 1.329.

1.3718 at 20" for water and acetic acid, respectively. Critical Tables."

were corrected according to Alex. Smith's value (4) for associated liquids.

Methanol-Acetone Free.

Acetone-free methanol was distilled from dilute hydrochloric acid and then once from commercial quick lime and 3 times from activated lime (2). 1500 cc. of this material was redistilled, the middle fraction of 500 cc. being collected. This sample was then subjected to fractionation as shown in the following table.

Fraction.

B. P. N%.

Fraction.