Variable temperature CP/MAS13C NMR study of cyclodextrin complexes of benzaldehyde
β Scribed by John A. Ripmeester
- Book ID
- 104869504
- Publisher
- Springer Netherlands
- Year
- 1988
- Tongue
- English
- Weight
- 484 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0923-0750
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A method for temperature calibration of CP/MAS NMR probes and their temperature controllers is described that relies upon known phase changes in the compounds adamantane, d-camphor, pivalic acid and DABCO. The method appears to give a convenient and reliable calibration over the temperature range cu
## Abstract ^13^C CP/MAS NMR spectra were recorded to characterize the solidβstate conformation of flavonoids: galangin, kaempferol, quercetin, myricetin, chrysin, apigenin, luteolin, acacetin, hesperetin and naringenin. Correct assignment of the signals in solutionβstate spectra (using APT, HSQC a