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Uvanite, a Swelling Uranyl Vanadate with a Layer Structure

โœ Scribed by Prof. Dr. Armin Weiss; Dipl.-Chem. K. J. Hilke

Publisher
John Wiley and Sons
Year
1965
Tongue
English
Weight
112 KB
Volume
4
Category
Article
ISSN
0044-8249

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โœฆ Synopsis

1.0-2.0 ppm due to the methylene and methine protons, and B singlet at 3.14 ppm due to the methoxy group. Heating of ethoxybenzene with HGeCI3 for 0.5 h at 110 to 1 3 0 ' C and subsequent methylation lead to t h e ethoxy derivatives corresponding to (3). I t is remarkable that the reaction of alkoxybenzenes and HGeCI3 docs not give rise to trichlorogermylbenzene, since refluxing of dialkyl ethers with HGeCI, produces alkyltrichlorogermanes in yields of 35-40

[l].

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