Utilization of bromination reactions for the determination of carbamazepine using bromate–bromide mixture as a green brominating agent
✍ Scribed by Basavaiah, Kanakapura; Abdulrahman, Sameer A.M.
- Book ID
- 120620046
- Publisher
- Elsevier
- Year
- 2014
- Tongue
- English
- Weight
- 626 KB
- Volume
- 7
- Category
- Article
- ISSN
- 1878-5352
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## Abstract In the presence of 2 mol‐equiv. of AcONa, both triglycosylborane **1** and dicyclohexylglycosylborane **2** readily react with bromine chloride generated __in situ__ from bromide and __N__‐chlorosuccinimide (NCS) to give the bromo‐sugar **3** (75 and 60%, resp.). The use of the BH~3~‐TH