✦ LIBER ✦

Using chemical shift anisotropy to resolve isotropic signals in solid-state NMR

✍ Scribed by Matthew S. Ironside; Robin S. Stein; Melinda J. Duer

Book ID: 108184848
Publisher: Elsevier Science
Year: 2007
Tongue: English
Weight: 442 KB
Volume: 188
Category: Article
ISSN: 1090-7807
DOI: 10.1016/j.jmr.2007.06.003

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Spectral Editing in Solid-State MAS NMR

Spectral Editing in Solid-State MAS NMR Using Chemical-Shift-Anisotropy-Dephasing Techniques

✍ J. Peng; L. Frydman 📂 Article 📅 1995 🏛 Elsevier Science 🌐 English ⚖ 285 KB

Assigning solid-state NMR spectra of ali

Assigning solid-state NMR spectra of aligned proteins using isotropic chemical shifts

✍ Anna A. De Angelis; Stanley C. Howell; Stanley J. Opella 📂 Article 📅 2006 🏛 Elsevier Science 🌐 English ⚖ 139 KB

Chemical Shift Anisotropy and Offset Eff

Chemical Shift Anisotropy and Offset Effects in Cross Polarization Solid-State NMR Spectroscopy

✍ Srinivasan C. Shekar; Dong-Kuk Lee; A. Ramamoorthy 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 270 KB

The effect of an offset term in the cross-polarization (CP) Hamiltonian of a heteronuclear spin-12 pair due to off-resonant radio frequency (rf) irradiation and/or chemical shift anisotropy on one of the rf channels is investigated. Analytical solutions, simulations, and experimental results are pre

Determination of Polypeptide Backbone Di

Determination of Polypeptide Backbone Dihedral Angles in Solid State NMR by Double Quantum 13C Chemical Shift Anisotropy Measurements

✍ Francisco J. Blanco; Robert Tycko 📂 Article 📅 2001 🏛 Elsevier Science 🌐 English ⚖ 238 KB

A solid state NMR technique for the determination of peptide backbone conformations at specific sites in unoriented samples under magic angle spinning (MAS) is described and demonstrated on a doubly labeled polycrystalline sample of the tripeptide AlaGlyGly and a sextuply labeled lyophilized sample

Relationship of chemical shift to glycos

Relationship of chemical shift to glycosidic conformation in the solid-state13C NMR spectra of (1 → 4)-linked glucose polymers and oligomers: anomeric and related effects

✍ Michael C. Jarvis 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 557 KB

Use of 13C chemical shift surfaces in th

Use of 13C chemical shift surfaces in the study of carbohydrate conformation. Application to cyclomaltooligosaccharides (cyclodextrins) in the solid state and in solution

✍ Edward P. O’Brien; Guillermo Moyna 📂 Article 📅 2004 🏛 Elsevier Science 🌐 English ⚖ 414 KB