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Use of C,N-chelated di-n-butyltin(IV) fluoride for the synthesis of acyl fluorides, fluoroformates and fluorophosgene

✍ Scribed by Petr Švec; Aleš Eisner; Lenka Kolářová; Tomáš Weidlich; Vladimír Pejchal; Aleš Růžička

Book ID
104095756
Publisher
Elsevier Science
Year
2008
Tongue
French
Weight
186 KB
Volume
49
Category
Article
ISSN
0040-4039

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✦ Synopsis

Dedicated to Prof. Dr. Rudolph Willem on the occasion of his 60th birthday in recognition of his outstanding contributions to the area of organometallic chemistry and NMR spectroscopy 1) reacts with various chloroformates, acyl chlorides, methanesulfonyl chloride, 4,4 0 -dimethoxytrityl chloride and phosgene precursors or derivatives to form fluorinated analogues. All reactions proceed rapidly and under mild conditions. The use of a catalytic amount of 1 and KF in toluene led to a relatively high yield of a selected fluoroformate.

📜 SIMILAR VOLUMES

ChemInform Abstract: Use of C,N-Chelated
ChemInform Abstract: Use of C,N-Chelated Di-n-butyltin(IV) Fluoride for the Synthesis of Acyl Fluorides, Fluoroformates and Fluorophosgene.
✍ Petr Svec; Ales Eisner; Lenka Kolarova; Tomas Weidlich; Vladimir Pejchal; Ales R 📂 Article 📅 2009 🏛 John Wiley and Sons ⚖ 40 KB

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