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Use of 13C-n.m.r. spectroscopy for the quantitative estimation of 3-O- and 3,6-di-O-substituted d-glucopyranosyl residues in α-d-glucans formed by the d-glucosyltransferases of Streptococcus sobrinus

✍ Scribed by Atsunari Shimamura

Book ID
107725792
Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
721 KB
Volume
185
Category
Article
ISSN
0008-6215

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Molecular structure of 3-O-(3,6-anhydro-
Molecular structure of 3-O-(3,6-anhydro-α-d-galactopyranosyl)-β-d-galactopyranose (neocarrabiose) in the solid state and in solution: an investigation by X-ray crystallography, n.m.r. spectroscopy, and molecular mechanics calculations
✍ Doriano Lamba; Anna Laura Segre; Steven Glover; William Mackie; Bernard Sheldric 📂 Article 📅 1990 🏛 Elsevier Science 🌐 English ⚖ 936 KB

The crystal structure of neocarrabiose monohydrate, 3-O-(3,6-anhydro-alpha-D-galactopyranosyl)-beta-D-galactopyranose (C12H20O10.H2O) belongs to the monoclinic space group P2(1), and has a unit cell of dimensions a = 6.351(1), b = 7.675(2), c = 15.096(8) A, and beta = 91.11(1) degree. The reducing u