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Unusual Stepwise Assembly and Molecular Growth: [H14Mo37O112]14− and [H3Mo57V6(NO)6O189(H2O)12(MoO)6]21−

✍ Scribed by Achim Müller; Jochen Meyer; Erich Krickemeyer; Christian Beugholt; Hartmut Bögge; Frank Peters; Marc Schmidtmann; Paul Kögerler; Michael James Koop

Publisher: John Wiley and Sons
Year: 1998
Tongue: English
Weight: 330 KB
Volume: 4
Category: Article
ISSN: 0947-6539
DOI: 10.1002/(sici)1521-3765(19980615)4:6<1000::aid-chem1000>3.0.co;2-c

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The blue mixed-crystal title compound Na 15 [Mo VI 126 Mo V 28 O 462 H 14 (H 2 O) 70 ] 0.5 [Mo VI 124 Mo V 28 O 457 H 14 (H 2 O) 68 ] 0.5 ´ca. 400 H 2 O º Na 15 [1 a] 0.5 [1 b] 0.5 ´ca. 400 H 2 O 1, which crystallizes in the triclinic space group P 1 (a = 30.785(2), b = 32.958(2), c = 47.318(3) A Ê