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Unusual (but precedented) equilibrium between 1,4- and 1,6-Di(2- hydroxyethyl)cyclooctatetraene

✍ Scribed by Marshall R. Gottesfeld; Frederick A. Masoudi; David E. Hansen

Book ID
108382327
Publisher
Elsevier Science
Year
1992
Tongue
French
Weight
193 KB
Volume
33
Category
Article
ISSN
0040-4039

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✍ Rolf Sigrist; Hans-Jürgen Hansen 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 German ⚖ 412 KB

## Abstract The oxidation of 1‐(3,8‐dimethylazulen‐1‐yl)alkan‐1‐ones **1** with 2,3‐dichloro‐5,6‐dicyano‐1,4‐benzoquinone (=4,5‐dichloro‐3,6‐dioxocyclohexa‐1,4‐diene‐1,2‐dicarbonitrile; DDQ) in acetone/H~2~O mixtures at room temperature does not only lead to the corresponding azulene‐1‐carboxaldehy