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Unusual amino acids. 5. Synthesis of 3,5-dioxopyrazolidine derivatives

✍ Scribed by D. Zicane; Z. Tetere; I. Rijkure; M. V. Petrova; E. Gudriniece; U. Kalejs


Book ID
105516695
Publisher
Springer US
Year
2000
Tongue
English
Weight
209 KB
Volume
36
Category
Article
ISSN
0009-3122

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Ketene dithioacetal derivatives of 1-phe
✍ Aurora Molinari; Alfonso Oliva; LucΓ‘ SΓ‘nchez; Arturo San Feliciano πŸ“‚ Article πŸ“… 1997 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 213 KB

## Abstract 1‐Phenyl‐3,5‐dioxopyrazolidine 1 reacts with carbon disufide and alkyl halides in presence of excess of sodium acetate in dimethylformamide to afford the ketene dithioacetals 3a‐h. The ^13^C chemical shift assignments of these compounds were made on the basis of two‐dimensional nmr stud