Untersuchungen zur Sulfochlorierung von Paraffinen. X. Über die Anwendbarkeit additiver Inkremente bei der Auswertung der 13C-NMR-Spektren von Alkanmono- und -disulfochloriden und von Chloralkansulfochloriden
✍ Scribed by Dr. habil. R. Radeglia; Dr. W. Schmidt-Renner
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- English
- Weight
- 321 KB
- Volume
- 323
- Category
- Article
- ISSN
- 1615-4150
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✦ Synopsis
Studies on Sulphochlorination of Paraffins. X. The Application of Additive Increments for the Interpretation of ^13^C‐N.M.R. Spectra of Alkane Mono‐ and Disulphochlorides and of Chloroalkane Sulphochlorides
Increments which consider the influence of chlorine and sulphonylchloride substituents on the ^13^C‐n.m.r. shifts of alkanes were calculated and discussed. The application of additive increments for the calculation of ^13^C‐n.m.r. chemical shifts of alkane‐1,2‐disulphonylchlorides, branched alkane monosulphonylchlorides, sulphochlorinated 1‐alkylchlorides and chlorinated 1‐alkane sulphonylchlorides is demonstrated. The limitations of the method are discussed.