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Unresolvable long range spin–spin coupling as a source of systematic error in proton NMR total bandshape analysis

✍ Scribed by Torbjörn Drakenberg; Robert E. Carter


Publisher
John Wiley and Sons
Year
1975
Tongue
English
Weight
218 KB
Volume
7
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

Unresolvable long range spin‐spin coupling which is not explicitly taken into account in total NMR bandshape analysis is demonstrated to be a potentially important source of systematic error, leading to Δ__H__^≠^ and δ__S__^≠^ values incorrect by c. 1 kcal/mol and 2 to 4 cal/(mol K), respectively.