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Unprecedented Association of [Mo6Br7iYiBr6a]3- Cluster Units and [MoIIIBr6]3- Complexes: Synthesis, Crystal Structures, and Properties of the Double Salts Rb3 [Mo6Br7iYiBr6a](Rb3[MoBr6])3 (Y: Se, Te).

✍ Scribed by Kaplan Kirakci; Stephane Cordier; Christiane Perrin


Publisher
John Wiley and Sons
Year
2006
Weight
10 KB
Volume
37
Category
Article
ISSN
0931-7597

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K 2 W 6 Br 14 (I), Rb 2 W 6 Br 14 (II), and Cs 2 W 6 Br 14 (III) were formed by reactions of W 6 Br 12 with the corresponding alkali metal bromides in evacuated silica tubes with a temperature gradient of 925 K/915 K. (I) crystallizes in the cubic space group Pn3 (no. 201), a = 13.808 A Ê , Z = 4, c