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Unexpected result of the reaction of 2-vinyloxyethyl isothiocyanate with bromoacetic acid

✍ Scribed by N. A. Nedolya; N. P. Papsheva; A. V. Afonin; B. A. Trofimov; V. A. Kukhareva; T. V. Kashik

Book ID
112450024
Publisher
Springer
Year
1991
Tongue
English
Weight
135 KB
Volume
40
Category
Article
ISSN
1573-9171

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## Abstract Unexpectedly, in the reaction of 2‐bromo‐2‐phenylacetonitrile derivatives with 2β€…mol‐equiv. of benzothioamide in DMSO, 3,5‐diaryl‐1,2,4‐thiadiazoles were obtained in excellent yields (83–90%) and in short reaction times (5–10β€…min). It is found that, in DMF, a quite different reaction ta