✦ LIBER ✦
Unequivocal assignment of the fullerene carbons of diethyl 1,2-methano[60]fullerene 61,61-dicarboxylate using 2D INADEQUATE NMR spectroscopy
✍ Scribed by Glenn A. Burley; Paul A. Keller; Stephen G. Pyne; Graham E. Ball
- Book ID
- 102527042
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- English
- Weight
- 168 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.879
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✦ Synopsis
Abstract
Assignment of all carbons of the [60]fullerene sphere of diethyl 1,2‐methnano[60]fullerene 61,61‐dicarboxylate using 2D INADEQUATE NMR spectroscopy is described. Acquiring the INADEQUATE data with small spectral widths and optional F~1~ folding with States‐TPPI phase implementation provides a convenient route to high‐resolution data. A description of the topology of the [60]fullerene sphere and its comparison with x‐ray crystallographic analysis is also presented. Copyright © 2001 John Wiley & Sons, Ltd.