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Two-phase derivatization of pentazocine with chloroformate esters and determination by gas chromatography

✍ Scribed by Per Hartvig; Christina Fagerlund; Ulf Bondesson


Book ID
103910625
Publisher
Elsevier Science
Year
1984
Tongue
English
Weight
698 KB
Volume
2
Category
Article
ISSN
0731-7085

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## Abstract The derivatization method of thiazolidine‐4‐carboxylic acid (TZCA) and methyl‐thiazolidine‐4‐carboxylic acid (Me‐TZCA) in urine with alcohol/chloroformate was achieved. TZCA and Me‐TZCA were derivatized in one step in urine with ethyl chloroformate in 1 min at room temperature. The deri