This communication describes the use of two-dimensional relayed (TOCSY)-ROESY experiments for the rapid and selective identification of alpha/beta1,2-glycosidic linkages in polysaccharides. The method assists in the identification of cross-peaks in crowded regions of ROESY spectra by moving them to
Two-dimensional NMR spectroscopy of glycosides
β Scribed by Hans C. Krebs; Gerhard G. Habermehl
- Publisher
- John Wiley and Sons
- Year
- 1992
- Tongue
- English
- Weight
- 245 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0749-1581
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β¦ Synopsis
Abstract
Twoβdimensional NMR spectroscopy was used for the structure elucidation of glycosides. In particular, the connectivity between different sugar residues and between sugar and acid moieties is discussed.
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