✦ LIBER ✦

Two-dimensional magic-angle-spinning NMR of partially ordered systems

✍ Scribed by O.S. Harbison; H.W. Spiess

Publisher: Elsevier Science
Year: 1986
Tongue: English
Weight: 694 KB
Volume: 124
Category: Article
ISSN: 0009-2614
DOI: 10.1016/0009-2614(86)85131-4

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✦ Synopsis

A new two-dimensional NMR experiment is presented, which, when applied to rotor-synchronised magic-angle-spinning spectra of partially ordered solids, gives information both on the chemical shielding tensor orientation and on the degree of order in the sample, e.g., in partially ordered synthetic or biopolymers.

Application of the experiment is demonstrated using samples of highly oriented polyethylene.

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