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Tritium nuclear magnetic resonance spectroscopy. Distribution patterns and nuclear overhauser enhancements in some tritiated steroids

✍ Scribed by Lawrence J. Altman; Norman Silberman


Book ID
118978373
Publisher
Elsevier Science
Year
1977
Tongue
English
Weight
356 KB
Volume
29
Category
Article
ISSN
0039-128X

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Tritium nuclear magnetic resonance spect
✍ Jasim M. A. Al-Rawi; John A. Elvidge; John R. Jones; Victor M. A. Chambers; Anth πŸ“‚ Article πŸ“… 1976 πŸ› John Wiley and Sons 🌐 French βš– 322 KB πŸ‘ 1 views

## Abstract The usefulness of ^3^H n.m.r. spectroscopy as an analytical tool for the determination of tritium distribution in both generally and specifically labelled compounds is illustrated by reference to the results for phenylalanine and several other amino acids.

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## Abstract Pyridine, methylpyridines, quinoline and isoquinoline have been labelled with deuterium using pre‐reduced platinum dioxide (PtO~2~Β·2H~2~O) and heavy water. Their ^2^H chemical shifts from monodeuteriated TMS have been assigned. The extent of the labelling has been determined directly by