𝔖 Bobbio Scriptorium
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Tritium Labelling of Cyprodime ( = (—)-17-(Cyclopropylmethyl)-4,14-dimethoxymorphinan-6-one), a μ Receptor-Selective Opioid Antagonist

✍ Scribed by Ferenc Ötvös; Géza Tóth; Helmut Schmidhammer


Publisher
John Wiley and Sons
Year
1992
Tongue
German
Weight
169 KB
Volume
75
Category
Article
ISSN
0018-019X

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✦ Synopsis


Abstract

The preparation of [1‐^3^H]cyprodime (2), which has a specific activity of 31.6 Ci/mmol was carried out by catalytic tritiodehalogenation of 1‐bromocyprodime (3). Bromination of cyprodime was performed by using chloroperoxidase, KBr, and H~2~O~2~.