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Tritium labelling and tritium N.M.R. - part I alpha-labelled stearic, palmitic, myristic and lauric acids

✍ Scribed by P. C. Crossley; R. W. Martin; J. B. Mawson; A. L. Odell


Publisher
John Wiley and Sons
Year
1980
Tongue
French
Weight
198 KB
Volume
17
Category
Article
ISSN
0022-2135

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✦ Synopsis


Abstract

Stearic, palmitic, myristic and lauric acids have been labelled with tritium in the alpha carbon position, and the position of the label confirmed using tritium N.M.R. spectrometry. The α‐^3^H acids were prepared using tritiated water with sulphuric acid or sodium hydroxide as catalysts. Specifically labelled compounds of high specific activity and radiochemical purity were obtained.