Tri­phenyl­boroxin complex with N-cyclo­hexyl­hydroxy­lamine and its isobutyr­aldehyde nitro­ne

✍ Scribed by Kliegel, Wolfgang ;Lubkowitz, Gottfried ;Patrick, Brian O. ;Rettig, Steven J. ;Trotter, James

• Book ID: 104479653
• Publisher: International Union of Crystallography
• Year: 2002
• Tongue: English
• Weight: 287 KB
• Volume: 58
• Category: Article
• ISSN: 1600-5368
• DOI: 10.1107/s1600536802015052

✦ Synopsis

N-Cyclohexylhydroxylamine(O±B)triphenylboroxin N-cyclohexyl-C-(2-propyl)nitrone hemibenzene hemisolvate, C 24 H 28 -B 3 NO 4 .C 10 H 19 NOÁ0.5C 6 H 6 , contains one molecule of Ncyclohexylhydroxylamine in its N-oxide form added to a boroxin heterocycle, with one molecule of N-cyclohexyl-C-(2propyl)nitrone linked by an OÁ Á ÁHÐN hydrogen bond to the protonated hydroxylamine moiety, and a molecule of benzene which is located on a centre of inversion.