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Triorganotin(IV) complexes containing multifunctional meso-dimercaptosuccinic acid ligand: Syntheses, characterizations, and crystal structures

✍ Scribed by Chunlin Ma; Qingfeng Wang; Rufen Zhang

Publisher: John Wiley and Sons
Year: 2009
Tongue: English
Weight: 244 KB
Volume: 20
Category: Article
ISSN: 1042-7163
DOI: 10.1002/hc.20511

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✦ Synopsis

Four triorganotin complexes of the types [(R 3 Sn)

and R = PhCH 2 4) have been obtained by the reaction of meso-dimercaptosuccinic acid and sodium ethoxide with triorganotin(IV) chloride in 1:2:2 stoichiometry. All the complexes were characterized by elemental analyses, IR spectroscopy, and NMR spectroscopy. Furthermore, complexes 1 and 2 were characterized by X-ray diffraction analyses, which revealed that complexes 1 and 2 are mononuclear structures and further interlinked by intermolecular C H•••O and O H•••O hydrogen bonds, respectively.

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