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Trimerization of 1,4-Dichloro-2-butyne to 5-(1′-Chlorovinyl)-1,2,3,4,5-pentachloromethylcyclopentadiene (II) Catalyzed by Palladium Complex.

✍ Scribed by Jinsheng Cheng; Jinheng Li; Huanfeng Jiang; Xiaoyue Ouyang; Qunjian Zhang

Publisher: John Wiley and Sons
Year: 2003
Weight: 70 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200350083

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## Abstract 1,2,4‐Triphenyl‐1,3,5‐triazapentadiene (1a), prepared from benzamidine and __N__‐phenylbenzimidoyl chloride, was treated at room temperature with CoCl~2~, Ni(NO~3~)~2~, Na~2~PdCl~4~, CuCl~2~ and ZnCl~2~ to form the corresponding six‐membered 1:1 chelate complexes 1a·CoCl~2~, 1a·Ni(NO~3~