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Triazoles. Part III. Mono- and di-methyl(phenyl)-1 : 2 : 4-triazoles

✍ Scribed by Atkinson, M. R. ;Polya, J. B.


Book ID
127293345
Publisher
The Royal Society of Chemistry
Year
1954
Weight
560 KB
Category
Article
ISSN
0368-1769

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The title compound, C 21 H 19 N 5 , has been synthesized and characterized by single-crystal X-ray diffraction. The dihedral angle between the benzene and triazole rings is 123.0 (5) . The triazole ring forms dihedral angles of 36.5 (5) and 50.1 (5) with the two pyridyl rings.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.045 wR factor = 0.125 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 14 H 12 N 4 , is a disubstituted 1,2,4-triazole derivative. The triazole ring is planar and its dihedral angles with the attached pyridyl and methylphenyl rings are 25.2 (3) and 66.9 (3) , respectively. The crystal structure is stabilized by a number of CÐHÁ Á ÁN hydrogen bonds