Triammonium nonaiododiantimonate(III), (NH4)3[Sb2I9]
✍ Scribed by Zhang, Hui ;Fang, Liang ;Yuan, Run-Zhang
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 261 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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Preparation and Crystal Structure of Triammonium-trisulfimide (NH 4 ) 3 (NSO 2 ) 3 . -The structure of (I) is determined by powder and single crystal XRD (space group P2 1 /c, Z = 4). The structure determination reveals a chair-conformation of the anions, which are arranged to form a hexagonal rod
Proton magnetic resonance second moment and spin-lattice relaxation time were carried out on polycrystalline tris (n-propylammonium) enneachlorodiantimonate (III), (n-C,H,NH,),Sb,Cl,, in the temperature range of lo-370 K. The second moment measurements show that the structure is not rigid on the NMR