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Trialkylsilyl esters of polyfluoroacylphosphonic acids

โœ Scribed by V. M. D'yakov; M. G. Voronkov

Book ID
112421597
Publisher
Springer
Year
1973
Tongue
English
Weight
280 KB
Volume
22
Category
Article
ISSN
1573-9171

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Stereoselective formation of silylketene
Stereoselective formation of silylketene acetals from esters and trialkylsilyl perchlorates.
โœ Craig S. Wilcox; Robert E. Babston ๐Ÿ“‚ Article ๐Ÿ“… 1984 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 212 KB

Alkanoate esters react with triethylsilyl perchlorate and trialkylamines at low temperature to yield 0-silylketene acetals. The 2 isomer is obtained in excellent yield. ## 1 Silylketene acetals find frequent application in carbon-carbon bond forming reactions. One approach to silylketene acetals