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Transition Metal-Catalyzed Asymmetric Hydroamination of Alkenes (AHA)

✍ Scribed by Kai C. Hultzsch

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
368 KB
Volume
347
Category
Article
ISSN
1615-4150

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The thiophosphinic amide 2 was prepared in 68 % yield by the reaction of 2,2-dimethyl-1,3-propanediamine with diisopropylchlorophosphine followed by the addition of sulfur. Attachment of the proligand 2 to zirconium was achieved by direct metalation with ZrA C H T U N G T R E N N U N G (NMe 2 ) 4 in