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Transformation of Carotol into the Hydroindane-Derived Musk Odorant

✍ Scribed by Jozef Kula; Radoslaw Bonikowski; Maria Staniszewska; Arkadiusz Krakowiak; Michal W. Wieczorek; Wieslaw R. Majzner; Grzegorz D. Bujacz

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 104 KB
Volume: 2002
Category: Article
ISSN: 1434-193X
DOI: 10.1002/1099-0690(200206)2002:11<1826::aid-ejoc1826>3.0.co;2-a

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✦ Synopsis

Ozonolysis of carotol (1) gives dihydroxy ketone 2 (63% yield), the absolute configuration of which was established by X-ray crystallography. An acidic dehydration of 2 delivers a mixture of isomeric ketones 3 and 4 (3:1) that, catalysed by

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