Transfer of acetone between a continuous aqueous phase and dispersed organic phase in a packed column
โ Scribed by T.E. Degaleesan; G.S. Laddha
- Publisher
- Elsevier Science
- Year
- 1966
- Tongue
- English
- Weight
- 336 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0009-2509
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โฆ Synopsis
This length corresponds to a certain time taken by the fluid to adjust its velocity profile, and if in pulsed flow the period of the pulsations is much greater than the adjustment time, then the quasi-steady state assumption is valid. The condition for validity can be written:
In the present work a was in the range 6.7-10, so the quasisteady assumntion is hardly valid. It is likely (a) that turbulent conditions persisted in the-water even when the instantaneous Reynolds number was less than 2000 and (b) that some of the eddies generated at velocity peaks persisted during the slower parts of the cycle. Effect (b) may account for the unexpected positive effect of pulsation at low values of Y.
From the practical point of view, it is concluded that pulsations will improve heat transfer in the turbulent flow regime, particularly if the flow can be made to reverse in direction for part of the cycle, The maximum improvement ratio obtained was R = 1.41, on the basis of the overall heat transfer coefficient. The corresponding improvement in the water-side coefficient may be estimated from Eq. ( 3) for Y = I and n = 0.8 to give R = 3.25. In future work it would be desirable to measure the tube wall temperature and thereby directly obtain a value for the water-side heat transfer coefficient.
๐ SIMILAR VOLUMES
An experimental study with three different heterogeneous azeotropic mixtures (acetone/toluene/water, 1-propanol/1-butanol/ water and ethanol/cyclohexane/water) has been carried out with the object to analyze the separation efficiency of three-phase distillation in a packed column. The experiments we
Packed bed hollow fiber membrane reactors were used to carry out organic phase biocatalysis at constant water activity. The performance of the device was tested by carrying out the esterification of dodecanol and decanoic acid in hexane. Lipase from Candida rugosa, immobilized on microporous polypro