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Traceless solid phase synthesis of 2-substituted pyrimidines using an ?off-the-shelf? chlorogermane-functionalised resinElectronic supplementary information (ESI) available: experimental procedures and key data for all the reactions described. See http://www.rsc.org/suppdata/ob/b3/b303064d/

✍ Scribed by Spivey, Alan C.; Srikaran, Ratnasothy; Diaper, Christopher M.; Turner, David J.

Book ID: 120213797
Publisher: Royal Society of Chemistry
Year: 2003
Tongue: English
Weight: 144 KB
Volume: 1
Category: Article
ISSN: 1477-0520
DOI: 10.1039/B303064D

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1H-1,3-Diazepines, 5H-1,3-diazepines, 1,3-diazepinones, and 2,4-diazabicyclo[3.2.0]heptenesPreliminary reports on parts of this work have been published in ref 1. This paper is Diazepines, Part 3. For Part 2, see ref 2.,Electronic supplementary information (ESI) available: NMR spectra of 4a, 4c, 19v ? 20, 19a ? 25a, and 19g ? 25g (Fig. S1?S6), Arrhenius and Eyring plots for H-exchange in 4b,c (Fig. S7), views of the X-ray crystal structures of compounds 26 and 22bB (Fig. S8?S9), bond lengths and angles for compounds 4k, 22bB and 26, preparative procedures and characterization data for all compounds not described in the Experimental section, and computational data (Cartesian coordinates, absolute energies, IR, 1H and 13C NMR) for 20a?c, 21a?b, 22aA?F and 22aB dimer. See http://www.rsc.org/suppdata/ob/b3/b317099c/

✍ Reisinger, Ales; Koch, Rainer; Bernhardt, Paul V.; Wentrup, Curt 📂 Article 📅 2004 🏛 Royal Society of Chemistry 🌐 English ⚖ 496 KB