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Toward (+)-pancratistatin: Modulation of mechanism in an intramolecular electrophilic aromatic substitution

✍ Scribed by Timothy J. Doyle; Donald VanDerveer; John Haseltine

Book ID: 103403959
Publisher: Elsevier Science
Year: 1995
Tongue: French
Weight: 187 KB
Volume: 36
Category: Article
ISSN: 0040-4039
DOI: 10.1016/0040-4039(95)01248-g

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## Abstract Reaction rates for the protodesilylation of trimethylphenylsilane and of [2,4,6‐^2^H~3~]‐trimethylphenylsilane by HCIO~4~, were measured in aqueous methanol (2:5, __v/v__) and the secondary deuterium isotope effect for the reaction was found to be __k__~H~/__k__~D3~ = 0.79. The magnitud