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Total Synthesis of the Chlorinated Marine Natural Product Dysamide B.

✍ Scribed by Amanda C. Durow; G. Cliona Long; Susan J. O'Connell; Christine L. Willis

Publisher
John Wiley and Sons
Year
2007
Weight
14 KB
Volume
38
Category
Article
ISSN
0931-7597

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✍ Xiaochuan Chen; Jieping Zhu πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 153 KB πŸ‘ 2 views

Scheme 5. Domino cyclization to construct the pentacyclic core of cribrostatin 4 (1): a) n-C 6 H 13 SH, TFA/TFE 1:100, 93 %; b) Swern oxidation; c) TBAF, AcOH, THF; d) MeSO 3 H (0.01 % by volume, c = 0.01 m), CH 2 Cl 2 , 51 % (for 3 steps). TFA = trifluoroacetic acid, TFE = trifluoroethanol.