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Total Synthesis of Hematoporphyrin and Protoporphyrin: A Conceptually New Approach

โœ Scribed by Martin, Pierre; Mueller, Markus; Flubacher, Dietmar; Boudier, Andreas; Blaser, Hans-Ulrich; Spielvogel, Dirk

Book ID
121840140
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
286 KB
Volume
14
Category
Article
ISSN
1083-6160

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Total Synthesis of Hematoporphyrin and P
Total Synthesis of Hematoporphyrin and Protoporphyrin: A Conceptually New Approach
โœ Martin, Pierre; Mueller, Markus; Flubacher, Dietmar; Boudier, Andreas; Blaser, H ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› American Chemical Society ๐ŸŒ English โš– 286 KB

The total synthesis of protoporphyrin IX and its disodium salt using a new alternative method to the classical MacDonald condensation is reported. The key step is the reaction of the new unsymmetrical diiodo dipyrrylmethane 1 with the known dipyrrylmethane 2. Coupling of the two fragments leads dire