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Total Synthesis of Cystothiazoles A and C

✍ Scribed by Williams, David R.; Patnaik, Samarjit; Clark, Michael P.

Book ID: 120025388
Publisher: American Chemical Society
Year: 2001
Tongue: English
Weight: 105 KB
Volume: 66
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo0106905

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ChemInform Abstract: Total Synthesis of

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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v

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Palladium-catalyzed cyclization-methoxycarbonylation of (2R,3S)-3-methylpenta-4-yne-1,2-diol (7) derived from (2R,3S)-epoxy butanoate 8 followed by methylation gave the tetrahydro-2-furylidene acetate (-)-9, which was converted to the left-half aldehyde (+)-4. A Wittig reaction between (+)-4 and the