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Total Synthesis of (+)-Azaspiracid-1. Part II: Synthesis of the EFGHI Sulfone and Completion of the Synthesis

✍ Scribed by David A. Evans; Travis B. Dunn; Lisbet Kværnø; André Beauchemin; Brian Raymer; Edward J. Olhava; Jason A. Mulder; Martin Juhl; Katsuji Kagechika; David A. Favor

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
339 KB
Volume
119
Category
Article
ISSN
0044-8249

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Total Synthesis of (+)-Azaspiracid-1. Pa
Total Synthesis of (+)-Azaspiracid-1. Part II: Synthesis of the EFGHI Sulfone and Completion of the Synthesis
✍ David A. Evans; Travis B. Dunn; Lisbet Kværnø; André Beauchemin; Brian Raymer; E 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 341 KB 👁 2 views

## Dedicated to Professor Dieter Seebach on the occasion of his 70th birthday With a practical synthesis of the ABCD aldehyde in hand (2, Scheme 1), [1] herein we describe our progress that culminated in the synthesis of (+)-azaspiracid-1 (1) in 26 linear steps and 2.7 % overall yield. As outline