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Total Synthesis of Apoptolidin: Part 1. Retrosynthetic Analysis and Construction of Building Blocks

✍ Scribed by K. C. Nicolaou; Yiwei Li; Konstantina C. Fylaktakidou; Helen J. Mitchell; Heng-Xu Wei; Bernd Weyershausen

Publisher: John Wiley and Sons
Year: 2001
Tongue: English
Weight: 155 KB
Volume: 40
Category: Article
ISSN: 0044-8249
DOI: 10.1002/1521-3773(20011015)40:20<3849::aid-anie3849>3.0.co;2-m

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## Abstract The preparation of three building blocks required for the total synthesis of woodrosin I (**1**) is outlined, a complex resin glycoside bearing a macrolide ring which spans four of the five sugars of its oligosaccharide backbone. Key steps involve the enantioselective, titanium‐catalyze