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Total synthesis of altohyrtin A (spongistatin 1): an alternative synthesis of the CD-spiroacetal subunit

โœ Scribed by Ian Paterson; Mark J Coster

Publisher
Elsevier Science
Year
2002
Tongue
French
Weight
118 KB
Volume
43
Category
Article
ISSN
0040-4039

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๐Ÿ“œ SIMILAR VOLUMES

Studies in marine macrolide synthesis: S
Studies in marine macrolide synthesis: Synthesis of a C16๎—ธC28 subunit of spongistatin 1 (altohyrtin A) incorporating the CD-spiroacetal moiety
โœ Ian Paterson; Debra J Wallace; Karl R Gibson ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 270 KB

The C! 6-C28 ketone 3, containing the CD-spiroacetal of spongistatin 1 (1), was prepared in 17 steps from aldehyde 9. Both thermodynamic and kinetic conditions were explored for controlling the CD-acetal configuration.