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Total synthesis of actinomycin D(C1) via a ring-opening reaction of aziridine

✍ Scribed by K. Okawa; K. Nakajima; T. Tanaka

Book ID
112126281
Publisher
Journal of Heterocyclic Chemistry
Year
1980
Tongue
English
Weight
123 KB
Volume
17
Category
Article
ISSN
0022-152X

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Synthesis of [4-11C]amino acids via ring-opening of aziridine-2-carboxylates
✍ N. M. Gillings; A. D. Gee 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 French ⚖ 144 KB 👁 1 views

## Abstract Ring‐opening of __N__‐(__tert__‐butoxycarbonyl)aziridine‐2‐isopropyl carboxylate with no‐carrier‐added (n.c.a.) [^11^C]cyanide is reported. Following purification by HPLC, the protected D,L‐[4‐^11^C]__β__‐cyanoalanine was subsequently hydrolysed, to yield D,L‐[4‐^11^C]asparagine or D,L‐