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Tomographic imaging of trickle-bed reactors

✍ Scribed by N. Reinecke; D. Mewes


Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
540 KB
Volume
51
Category
Article
ISSN
0009-2509

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✦ Synopsis


Trickle-bed reactors are used tbr a number of different reaction applications in chemical engineering processing. Among these applications hydrodesulfufization and hydrotreatment are the most common. For certain operating parameters of the reactor, the flow through the packing becomes instable and the pulse flow regime is established, in this regime, the mass transfer as well as the pressure drop is increased. In order to be able to operate commercial plants safely in this operating regime, the physical reasons for the onset and the physical properties of the pulsing itself need to be known. The tn~e physical mechanisms are especially important since the experimental investigations are usually camed out in experimental thcilities much below technical size. hi order to iav,'estigate the pulse i'low in irregular packings, capacitance tomogtapily was used. The imaging frequency of the system is 100Hz and the spatial resolution 0,1%. The investigations were performed at ambiant pressure in a 120mm diameter plant using air ~md water as the gas and liquid phase, respectively. The results indicate a strong three-dimensional distribution of the gas and the liquid phase inside the column. The liquid rich zones, appearing to be plane fi-om the outside, show a notl-unifonn distribution inside the packing. Due to the small diaaneter of the colmnn an influence of the walls was determined, which will not be lbund in larger size technical scale plants.


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## Abstract Local and average partial wetting efficiencies in trickle‐beds have been directly measured by image processing and PIV analysis. Two different setups have been implemented: a vertical monolayer of pellets where the wetting structure and stability and also local velocity gradient are cha

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A steady-state, two-dimensional model for cocurrent gas and liquid flow in a trickle-bed reactor is described. The model includes gas-liquid interaction and isothermal, incompressible flow without phase change or chemical reaction. The momentum equation proposed by Saez and Carbonell is used, along