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Tin(II) Ethyl Hexanoate Catalyzed Precipitation Polymerization of ε-Caprolactone in Supercritical Carbon Dioxide

✍ Scribed by Bratton, Daniel; Brown, Malcolm; Howdle, Steven M.

Book ID: 120344261
Publisher: American Chemical Society
Year: 2005
Tongue: English
Weight: 115 KB
Volume: 38
Category: Article
ISSN: 0024-9297
DOI: 10.1021/ma0484072

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## Abstract By using less catalyst in the ring‐opening polymerization of ε‐caprolactone, a residual tin content of 5 ppm was reached without the need for additional purification. The initial amount of tin (II) 2‐ethylhexanoate [Sn(Oct)~2~] was varied using catalyst:monomer ratios of 1:1000, 1:10,00