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Time displacement rotational echo double resonance: Heteronuclear dipolar recoupling with suppression of homonuclear interaction under fast magic-angle spinning

โœ Scribed by Tim W.T. Tsai; Yun Mou; Jerry C.C. Chan

Book ID
113726411
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
359 KB
Volume
214
Category
Article
ISSN
1090-7807

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Recoupling of Heteronuclear Dipolar Inte
Recoupling of Heteronuclear Dipolar Interactions with Rotational-Echo Double-Resonance at High Magic-Angle Spinning Frequencies
โœ Christopher P Jaroniec; Brett A Tounge; Chad M Rienstra; Judith Herzfeld; Robert ๐Ÿ“‚ Article ๐Ÿ“… 2000 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 120 KB

Heteronuclear dipolar recoupling with rotational-echo doubleresonance (REDOR) is investigated in the rapid magic-angle spinning regime, where radiofrequency irradiation occupies a significant fraction of the rotor period (10 -60%). We demonstrate, in two model 13 C-15 N spin systems, [1-13 C, 15 N]