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TiCl4 promoted three component coupling reaction: A new method for the synthesis of functionalized tetrahydrofurans and tetrahydropyrans

โœ Scribed by Arun K. Ghosh; Reiko Kawahama

Publisher
Elsevier Science
Year
1999
Tongue
French
Weight
244 KB
Volume
40
Category
Article
ISSN
0040-4039

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General procedure: A flame-dried round-bottomed flask was charged with 4 (1 equiv) and the olefin cross partner (3.0 equiv). A rubber septum was attached, dichloromethane was added (0.2 ยฑ 0.3 n in 4), and argon was bubbled through the resultant solution for 10 min. Under a stream of argon, 3 (0.050